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Extra info for Custom PC (September 2015)
Nanni, “Low-Temperature Aqueous Synthesis: a statistical design of experiment approach”, Journal of the European Ceramic Society, 20 3 15-320 (2000). B. , “A new computer program for Rietveld analysis of X-Ray powder diffraction patterns”, Journal of Applied Crystallography, 14 149-151 (1981). A. A. Ring, “Fundamentals of crystallisation: kinetic effects on particle size distributions and morphology”, Chemical Engineering Science, 46 2389-2427 (1991). M. O’Bryan and J. Thomson, “ Phase equilibria in the Ti02-rich region of the system BaO-TiOZ”, Journal of the American Ceramic Society, 57 522 (1974).
It is evident from table I that the addition of 1 and 2 wt % ZrO2 improves the density of the sintered pieces. With 3 wt % 2 1 - 0 2 the increment in density with respect to BaTi03 without additions is not significant. In figure 4 the displacement curves when the temperature is raised for several ZrO2 concentrations can be seen. In figure 5 the corresponding dy/dt against temperature curves are presented. When 1 wt % 2 1 - 0 2 is added to BaTi03, two peaks appear; one at 1163 "C and other at 1210 "C.
2 for powders synthesized for 24 h at several temperatures. The peak splitting becomes apparent at -180 "C. The concentrations of the cubic and tetragonal phases, as determined by Rietveld analysis, is shown in Fig. 3 for powders synthesized for 24 h at temperatures between 80 "C and 240 "C. According to the data in Figs. 2 and 3, the appearance of the peak splitting for the powder synthesized at 180 "C corresponds to a tetragonal content of -10 wt%. Furthermore, at the highest synthesis temperature (240 "C), the concentration of tetragonal BaTi03 is only -30 wt%.